Adding a certain compound to certain chemical reactions, such as: 170112-66-0, name is 3,4,5-Trifluoroiodobenzene, belongs to iodides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 170112-66-0, Product Details of 170112-66-0
3, 4, 5-trifluorolactic jodoethane hydroxybenzenesulfonic (10.0g, 38.0mmol), ethyl acetate tribromoacetic difluoroaniline (23.1g, 114mmol) and dimethyl sulfoxide soln. (40 ml) of copper (2.90g, 45.6mmol) to 80 C 3 at a time. Ethyl acetate is added to the reaction mixture, by filtering the insoluble matter. The liquid water is poured, extracted with ethyl acetate. The extract is washed with saturated salt solution, and dried in an anhydrous sodium sulfate, a vacuum concentrator. Concentrated silica gel column chromatography (elution solvent: ethyl acetate/n-hexane = 1/10) by, colorless oily for compd. (yield 7.20g, yield 75%) is obtained.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 3,4,5-Trifluoroiodobenzene, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Hokko Chemical Industry Co., Ltd.; Suzuki, Jun; Kobayashi, Yuta; Morita, Motoaki; Ota, Shinya; Onoue, Shinji; Ono, Ryuta; (40 pag.)JP2016/84328; (2016); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com