Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 2043-57-4, name is 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane, A new synthetic method of this compound is introduced below., Recommanded Product: 2043-57-4
1/T,liy,2No.,2No.-Perfluorooctyl thiouronium iodide (5); In a 100 mL round bottomed flask, thiourea (1.13g, 14.8 mmol) was added to a stirred solution of lH,lH,2H,2H-perfluorooctyl iodide (3.62 mL, 14.8 mmol) in ethyl alcohol (14.0 mL). The mixture was left to reflux at 78C for 13 hours under a nitrogen atmosphere then cooled to room temperature. The solvent was removed under reduced pressure to reveal a cream/white solid (8.10 g, 14.7 mmol, quantitative yield). This was used in the next step without further purification.
The synthetic route of 2043-57-4 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; ISIS INNOVATION LIMITED; GOUVERNEUR, Veronique; BEJOT, Romain; WO2010/7363; (2010); A2;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com