Synthetic Route of 124700-41-0, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 124700-41-0, name is 2-Fluoro-5-iodobenzoic acid belongs to iodides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
The eighth compound (10.000 g, 37.592 mmol) was dissolved in 40 mL of dichloromethane and 1 mL of DMF, and stirred at room temperature. The oxalyl chloride (3.800 mL, 45.110 mmol) was dissolved in 10 mL of dichloromethane and added dropwise to the reaction system, and stirred at room temperature for 1 h. After the reaction is completed, the reaction solution is sparged.It was replaced with anhydrous toluene three times to obtain an oily liquid ninth compound.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-Fluoro-5-iodobenzoic acid, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Beijing Institute of Technology; Liang Jianhua; Ma Congxuan; (36 pag.)CN109942653; (2019); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com