Application of 627-31-6, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 627-31-6, name is 1,3-Diiodopropane(stabilized with Copper chip) belongs to iodides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
Compound 11 (65 mg, 0.1 mmol), 1,3-diiodopropane (88.8 mg, 0.3 mmol) was added to an 8 mL vial.DIPEA (diisopropylethylamine, 20 uL), acetonitrile (150 uL), and the reaction mixture was reacted at 80 C for 12 hours.The reaction solution was drained, washed with DCM, washed with saturated aqueousThe solid was washed with diethyl ether to give a white solid compound 12 (40 mg, yield = 38%)
The synthetic route of 1,3-Diiodopropane(stabilized with Copper chip) has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Chinese Academy Of Sciences Shanghai Organic Chemistry Institute; Shi Shiliang; Cai Yuan; Yang Xintuo; Li Feng; (67 pag.)CN109776422; (2019); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com