Electric Literature of 7681-82-5, These common heterocyclic compound, 7681-82-5, name is Sodium iodide, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
To a solution of 44.81 g of lithium chloride in acetone was added 151.19 g of sodium iodide(1.05: 1). After 1 hour reaction, the reaction was completed and the sodium chloride was filtered off. The filtrate was concentrated to dryness to obtain lithium iodide. After drying, 134.12 g (97.80%) of anhydrous lithium iodide Rate 98%. Steamed acetone recovery, in addition to water recycling. The conversion ratio of anhydrous lithium chloride and anhydrous sodium iodide was 1.05: 1, and the conversion rate of lithium iodide was higher than that of Example 1.
Statistics shows that Sodium iodide is playing an increasingly important role. we look forward to future research findings about 7681-82-5.
Reference:
Patent; Shandong Boyuan Pharmaceutical And Chemical Co., Ltd.; Li Chenglin; Wang Qingmin; Zhai Yongli; Chu Rongqiang; (8 pag.)CN106928268; (2017); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com