Reference of 98-61-3, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 98-61-3, name is 4-Iodobenzenesulfonyl chloride belongs to iodides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
To the ammonium hydroxide (5.0 mL) was added 4-iodo-benzenesulfonyl chloride (454.0 mg, 1.5 mmol). The resulting mixture was stirred at room temperature for 2 h and extracted with DCM (2 × 20.0 mL). The combined organic phase was dried over anhydrous Na2SO4, and concentrated to give 39 as a white solid (392.0 mg). 1H NMR (400 MHz, DMSO-d6): delta 7.98-7.96 (d, J = 8.6 Hz, 2H), 7.60-7.58 (d, J = 8.6 Hz, 2H), 7.45 (s, 2H).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 4-Iodobenzenesulfonyl chloride, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Liu, Kai; Rao, Wei; Parikh, Hardik; Li, Qianbin; Guo, Tai L.; Grant, Steven; Kellogg, Glen E.; Zhang, Shijun; European Journal of Medicinal Chemistry; vol. 47; 1; (2012); p. 125 – 137;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com