Discovery of 52548-63-7

According to the analysis of related databases, 52548-63-7, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 52548-63-7, name is 5-Fluoro-2-iodobenzoic acid, This compound has unique chemical properties. The synthetic route is as follows., Formula: C7H4FIO2

General procedure: 1-acetoxyethanephosphonate-5-fluoro -1, 2- […] -3-(1H)-one (AFBX (2)) of synthetic The flask 2-iodo-5-fluorobenzoate 1330 mg (5mmol), then adding acetic acid 40 ml agitated until uniform. 3-hydroxybenzoic acid (purity 65%)overload Chloropyridin 1590 mg (6mmol) at a time and then adding a 24 60 C. The reaction liquid is cooled to 0 C, ether is added. The precipitate is filtered by deposition, vacuum drying in 1-acetoxyethanephosphonate-5-fluoro -1, 2- […] -3-(1H)-one (AFBX (2)) 770 mg (yield 48%)is obtained.

According to the analysis of related databases, 52548-63-7, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Tokyo Chemical Industry Co., Ltd.; Togo, Hideo; Inuma, Masataka; Moriyama, Katsuhiko; Takatsuki, Kenichi; (9 pag.)JP2015/63501; (2015); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com