A common compound: 116632-39-4, name is 5-Bromo-2-iodotoluene, belongs to iodides-buliding-blocks compound, it can change the direction of chemical reaction, and react with certain compounds to generate new functional products. A new synthetic method of this compound is introduced below. 116632-39-4
In N2Gas purification system, the compound G dissolved in a solution of tetrahydrofuran and toluene (5: 1), Compound H-1 (0.9 equiv) was added.Potassium carbonate (4.4 eq.) Was dissolved in deionized water was added Pd (0.05 eq.).The mixture was refluxed and stirred for 24 hours at the temperature 80 .After completion of the reaction, the mixture was extracted with organic solvent, and removing the organic solvent.The resultant was passed through the column to obtain Compound I-1
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 116632-39-4, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; LG Display Co., Ltd.; Liang, Zhonghuan; Yin, Jiongchen; Lu, Xiaozhen; Yin, Dawei; Shen, Renai; Jin, Zunyan; (39 pag.)CN105524071; (2016); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com