Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 4387-36-4, name is 2-Iodobenzonitrile, A new synthetic method of this compound is introduced below., Product Details of 4387-36-4
Weigh 0.02 mM halogenated aromatic hydrocarbon in a reaction flask, add 1 mL of solvent, and fill the reaction flask with nitrogen.Deoxygenation was performed for 10 minutes and 15 yL of triethylamine was added during the deoxygenation.After that, the reaction vessel was sealed, placed over a light-emitting diode (LED) with a wavelength of 400 nm and a power of 0.5 W, and the reaction was stirred at room temperature for 12 hours.After that, the dehalogenation reaction yield was characterized by gas chromatography-mass spectrometry.The yield of o-phenylacetonitrile was 80.7percent, and the characterization results of the gas chromatography and mass spectrometry were shown in Figure 2. The halogenated aromatic hydrocarbon waso-Iodobenzeneacetonitrile, the solvent is tetrahydrofuran.
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.