Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 19094-56-5, name is 2-Chloro-5-iodobenzoic acid, This compound has unique chemical properties. The synthetic route is as follows., Computed Properties of C7H4ClIO2
5g of 2-chloro-5-iodobenzoic acid and 30mL of methylene chloride were added into a 100mL reaction flask under nitrogen atmosphere, and then 0.13g of N, N-dimethylformamide was added, and 2.7g Oxalyl chloride, incubated at the end of the reaction dropwise 1h, and then warmed to 35-40 C for 2-3hrs, after the end of the reaction vacuum distillation, steamed to solvent-free fractions, and then added 30mL dichloromethane vacuum distillation, to be dried residual oxalyl chloride , Pale yellow viscous substance 5.3g, is 2-chloro-5-iodobenzoyl chloride, yield 100%.
According to the analysis of related databases, 19094-56-5, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Chongqing Boteng Pharmaceutical Technology Co., Ltd.; Lin Wenqing; Zheng Hongjie; Lin Chuanhua; Shen Chenjian; Liu Shouxuan; (6 pag.)CN106316803; (2017); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com