Reference of 455-13-0, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 455-13-0, name is 4-Iodobenzotrifluoride, This compound has unique chemical properties. The synthetic route is as follows.
Multi function cap round bottom 4-trifluoromethyl-iodobenzene to 250 ml (5.00g, 18.38mmol), imidazole (1.75g, 25.73mmol), Copper iodide (0.70g, 3.68mmol), Cesium carbonate (11.98g, 36.76mmol), Dimethylformamide (120 ml) for inserting and removing, adaptation stirring time 24 in the curved reflection 110. After reaction, bleeding of the volatiles of decompressing to a cutting, residue column in hexane and a ethylacetate crow mart yes blood section. The again 3A compound (3.12g, 14.71mmol) a obtained.
The chemical industry reduces the impact on the environment during synthesis 4-Iodobenzotrifluoride. I believe this compound will play a more active role in future production and life.
Reference:
Patent; LG Display Co.,Ltd; Lee, Sung Jae; Yang, Jung Hwan; Choe, Hyung Jong; Bae, Suk Young; Haw, Hay Ryeong; Kim, Chun Gi; (30 pag.)KR2016/14205; (2016); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com