Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 7681-82-5, name is Sodium iodide, A new synthetic method of this compound is introduced below., Recommanded Product: 7681-82-5
General procedure: 74.4mg (0.133mmol) of 1a? and 201mg (1.34mmol) of NaI are added to a round bottom flask with a stir bar followed by 10ml of THF. A reflux condenser is attached and the flask is submerged in an oil bath and refluxed for 3h. Then the mixture is allowed to cool to room temperature and solvent is evaporated. The residue is extracted with CH2Cl2, sonicated, and filtered through Celite with CH2Cl2. The process was repeated 3 times to remove and sodium halide. The solvent is evaporated from the combined extracts
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Article; Walsh, Aaron P.; Brennessel, William W.; Jones, William D.; Inorganica Chimica Acta; vol. 407; (2013); p. 131 – 138;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com