Introduction of a new synthetic route about 35453-19-1

According to the analysis of related databases, 35453-19-1, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 35453-19-1, name is 5-Amino-2,4,6-triiodoisophthalic acid, This compound has unique chemical properties. The synthetic route is as follows., Application In Synthesis of 5-Amino-2,4,6-triiodoisophthalic acid

In step 1, the product formed after the reaction of the compound A and the iodine chloride is compound B, 100 g of the compound B and 150 g of phosphorus pentachloride are mixed in a vessel, the reaction temperature is controlled at about 30 degrees Celsius, and the reaction time is controlled at 40 minutes. After the reaction is completed, a small amount of a chlorinating agent needs to be added to the reaction vessel. The chlorinating agent may be hydrochloric acid, and about 20 g of hydrochloric acid is added. After reacting for 10 minutes, it is rinsed with water, and then filtered to obtain a compound C.

According to the analysis of related databases, 35453-19-1, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Hubei Tianshu Pharmaceutical Co., Ltd.; Liu Yunlong; (12 pag.)CN109293526; (2019); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com