Introduction of a new synthetic route about 51560-21-5

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Compound 8 (1.0 g, 2.56 × 10 -3 mol) was dissolved in dichloromethane (20 mL) and stirred in an ice-salt bath for 30 minutes.A 1.0 M solution of BBr3 in dichloromethane (6.14 mL, 6.14 × 10 -3 mol) was added to the solution, and the mixture was stirred overnight.afterwards,After adding deionized water to the reaction mixture until no white smoke is generated,Suction filtration was performed.The obtained solid is dried under vacuum,Compound 9 was obtained as a white solid (yield 0.81 g, 87.1%).

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1,4-Diiodo-2,5-dimethoxybenzene, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Tokyo Denki University; Adachi, Naoya; Nagahori, Tomomi; (27 pag.)JP2020/2024; (2020); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com