Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 112671-42-8, name is 4-Bromo-1-iodo-2-nitrobenzene, This compound has unique chemical properties. The synthetic route is as follows., SDS of cas: 112671-42-8
Phenylboronic acid (76.84 g, 630.2 mmol) as starting material dissolved in 2780 mL THF was added to the round bottom flask, 4-bromo-1-iodo-2-nitrobenzene (309.96 g, 945.3 mmol), Pd(PPh3)4 (36.41 g,31.5 mmol), K2CO3 (261.3 g, 1890.6 mmol) and water 1390 mL were added and the resulting mixture was stirred at 80 C. When the reaction was completed, the resulting mixture was extracted with water and CH2Cl2 and the organic layer was dried over MgSO4 and concentrated to a silica gel column, and the resulting compound was recrystallized to obtain product was 122.68 g (yield: 70%).
According to the analysis of related databases, 112671-42-8, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Duksan Neolux Co., Ltd.; Park, Hyung Kun; Lee, Sun Hee; Lee, Yun Suk; So, Ki Ho; Park, Jong Kwang; Jung, Yeon Suk; Moon, Sung Yun; Lee, Jung Wook; (48 pag.)KR101614738; (2016); B1;,
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