Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 25309-64-2, name is 1-Ethyl-4-iodobenzene, This compound has unique chemical properties. The synthetic route is as follows., Safety of 1-Ethyl-4-iodobenzene
In a 25 mL reaction flask, 3 mL of water, 0.5 mmol of 1-ethyl-4-iodobenzene, 1.0 mmol of DBH, and0.05mmol TBHP, after reacting at 60 C for 4h, add 2.0mmol sodium bicarbonate and 0.5mmol alpha-aminopyridine at 80 CAfter reacting for 2 hours, the reaction mixture was completed, ethyl acetate was added thereto, and brine was added and the organic phase was concentrated.Column chromatography gave 134 mg of a white solid.The yield was 84%.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 25309-64-2.
Reference:
Patent; Henan Normal University; Zhao Minghao; Ma Chunhua; Zhu Hong; Yang Xiao; Zeng Wenjie; (9 pag.)CN108822106; (2018); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com