Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 16355-92-3, name is 1,10-Diiododecane, This compound has unique chemical properties. The synthetic route is as follows., SDS of cas: 16355-92-3
General procedure: N,N,N,N?,N?,N?-Hexabutylhexanediammonium diiodide (Bu6-diquat-6), N,N,N,N?,N?,N?-hexabutyloctanediammonium diiodide (Bu6-diquat-8), and N,N,N,N?,N?,N?-hexabutyldecanediammonium diiodide (Bu6-diquat-10) were synthesized by nucleophilic substitutionof the corresponding diiodoalkane with tributylamine. In a typical synthesis, to an oven-dried,nitrogen-filled, two-necked flask equipped with a condenser and a magnetic stirrer were addeddehydrated ethanol and tributylamine (3 equiv). Subsequently, diiodoalkane (1 equiv) was slowlyadded into the mixture. This mixture was heated slowly to 90 C and kept at this temperature in darkwhile stirring. After 48 h, the solution was cooled to room temperature and then ethanol wasevaporated by a rotary evaporator, producing semi-solid. This semi-solid was purified byrecrystallization in ethanol and ethyl acetate. The recrystallized solid was washed with acetone orhexane and dried under atmospheric condition.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 16355-92-3.
Reference:
Article; Keoh, Sye Hoe; Chaikittisilp, Watcharop; Endo, Akira; Shimojima, Atsushi; Okubo, Tatsuya; Bulletin of the Chemical Society of Japan; vol. 90; 5; (2017); p. 586 – 594;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com