In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 61203-48-3, name is 2-Iodo-4,5-dimethoxybenzoic acid belongs to iodides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. name: 2-Iodo-4,5-dimethoxybenzoic acid
[C.] [N- (5-NITROQUINOLIN-4-YL)-N- [2- (N, N-DIMETHYLAMINO) ETHYL]-2-IODO-4,] 5- dimethoxybenzamide (8d). The acid chloride prepared from 3,4-dimethoxy-6- iodobenzoic acid [(985] mg, 3.2 mmol) was redissolved in 30 mL of anhydrous methylene chloride, and this solution was added to a solution [OF 7D] (500 mg, 1.9 mmol) and triethylamine (2.0 g, 20.0 mmol) in methylene chloride (20 mL), and the resulting mixture was stirred at reflux for 2 h to provide 1. [17 G (81 %) OF 8D] as a gum. The material was obtained as a mixture of atropisomers and was used as such without separation or further purification; HRMS calcd for [C22H23OSN4IH] [: 551.] 0792; found: 551.0791.
The synthetic route of 61203-48-3 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; RUTGERS, THE STATE UNIVERSITY; LAVOIE, Edmond, J.; RUCHELMAN, Alexander, L.; LIU, Leroy, F.; WO2004/14906; (2004); A2;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com