Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 6940-76-7, name is 1-Chloro-3-iodopropane, This compound has unique chemical properties. The synthetic route is as follows., Safety of 1-Chloro-3-iodopropane
Synthesis of compound 7c To a suspension of NaH (22 mg, 0.85 mmol) in DMF (2.0 mL) was added S1 (305 mg, 0.78 mmol)in DMF (1.5 mL). After 10 min at room temperature, S4a (0.20 mL, 1.53 mmol) was added to thismixture, and the reaction mixture was stirred at room temperature for 6 h, diluted with ether,washed with water and dried over Na2SO4. Purification by FCC (PE/EtOAc, 8 : 1) gave thechloride S5a (344 mg, 94%) as a yellow oil. 1H NMR (400 MHz, CDCl3) delta 7.81 (d, J = 1.8 Hz,1H), 7.80 (d, J = 7.9 Hz, 1H), 7.24 (dd, J = 1.8, 7.9 Hz, 1H), 3.74 (s, 6H), 3.54 (t, J = 6 Hz, 2H),3.23 (s, 2H), 1.98-1.94 (m, 2H), 1.80-1.73 (m, 2H); 13C NMR (100 MHz, CDCl3) delta 170.6, 151.7,143.4, 142.6, 130.6, 125.3, 86.3, 58.4, 52.7, 44.4, 37.9, 30.3, 27.6.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 6940-76-7.
Reference:
Article; Gao, Yan; Shan, Dong; Jia, Yanxing; Tetrahedron; vol. 70; 34; (2014); p. 5136 – 5141;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com