Electric Literature of 172681-47-9, The chemical industry reduces the impact on the environment during synthesis 172681-47-9, name is 2-Amino-6-iodotoluene, I believe this compound will play a more active role in future production and life.
N-Acetyl-3-Iodo-2-Methyl Aniline Charge a 5 L, 3 neck flask equipped with a mantle, stirrer, condenser, with 708 grams (5M) 3-Iodo-2-Methyl Aniline, followed by 700 ml glacial acetic acid. Add in a stream of 520 grams (5.1M) acetic anhydride and allow the solution to come to a gentle reflux for an hour. The solution is allowed to cool and poured in a stream in a large container of 8 L ice water. The product will crystallize immediately and is filtered and squeezed under vacuum and air-dried. Yield was 900 grams (Theoretical yield=918 g).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-Amino-6-iodotoluene, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Latham, Keith R.; (67 pag.)US2018/117164; (2018); A1;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com