Simple exploration of

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 229178-74-9, name is 2,6-Difluoro-3-iodobenzoic acid, A new synthetic method of this compound is introduced below., SDS of cas: 229178-74-9

EXAMPLE 36A; Preparation of compound 2002; Step 1:; Sulfuric acid (3 mL) is added to a solution of 36a1 (15.0 g, 36.9 mmol) in MeOH (200 mL) and the resulting solution is stirred overnight at 800C. The mixture is cooled to RT, concentrated under reduced pressure, diluted with EtOAc (300 mL), washed with aqueous saturated sodium bicarbonate (3 x 100 mL), brine (100 mL), dried over Na2SO4, filtered and concentrated under reduced pressure to afford methyl ester 36a2.

The synthetic route of 229178-74-9 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; BOEHRINGER INGELHEIM INTERNATIONAL GmbH; WO2009/76747; (2009); A1;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com