Related Products of 83863-33-6,Some common heterocyclic compound, 83863-33-6, name is 5-Iodo-2-methylaniline, molecular formula is C7H8IN, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
solution of 5-iodo-2-methyl-phenylamine (20.4 g, 87.6 mmol) in 200 mL of dry CH2Cl2 was cooled to 0 C and acetic anhydride (16.5 mL, 175 mmol) was added dropwise. The mixture was heated to 50 C for 2 h and then cooled to 22 C. The resulting white precipitate was filtered to give c (18.4 g, 76%): MS m/z = 276 (M+H).
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route 5-Iodo-2-methylaniline, its application will become more common.