In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 2043-57-4 as follows. Recommanded Product: 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
In the first step, a fluorinated phosphonium salt was synthesized by reacting TPP and 2-perfluorohexyl ethyl iodide accordinto literature procedures [38,39]. Briefly, the fluorinated phosphonium salt was prepared by reacting TPP and fluoroalkyl iodide at 95 C in the absence of solvent. The reaction was continued for 24 h until all of the mixture was solidified. After cooling the resulting solid was washed several times with toluene and ether respectively. Then the white solid was dried at 50 C under vacuum.
According to the analysis of related databases, 2043-57-4, the application of this compound in the production field has become more and more popular.