Electric Literature of 7425-53-8, The chemical industry reduces the impact on the environment during synthesis 7425-53-8, name is Ethyl 4-iodobutanoate, I believe this compound will play a more active role in future production and life.
Add K2S2O5(3.0 equiv), Na2HPO4(2.0 equiv) and p-phenylstyrene (0.2 mmol) to thereaction tube in sequence, replace the air in the test tube with high-purity nitrogen and add 2 mL of DMF Solvent.Then, ethyl 4-iodobutyrate (4.0 equiv), triisopropylsilane (2.0 equiv) were added sequentially with a micro sampler, and stirred at 50 C for 24 hours.After the reaction was completed, the reaction solution was diluted with EA, extracted with water and saturated brine, respectively, and then the organic layer was dried, concentrated and separated by column chromatography to obtain the corresponding 1,2-bissulfone group-substituted compound 3c in 58% yield.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, Ethyl 4-iodobutanoate, other downstream synthetic routes, hurry up and to see.