Adding a certain compound to certain chemical reactions, such as: 627-31-6, name is 1,3-Diiodopropane(stabilized with Copper chip), belongs to iodides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 627-31-6, COA of Formula: C3H6I2
In a 25 mL flask, xanthene (1, 350 mg, 1.92 mmol),dissolved in dry THF (10 mL) and diiodopropane (0.2 mL 1.74 mmol) were stirred under argon at 0 C. n-Butyllithium (1 mL, solution 2.5 M in hexanes) was added dropwise, after which the reactionwas heated up to room temperature. After approx 2 h (TLC 40% hexane-CHCl3 7:3), solvent was evaporated in vacuo. The crude product was dissolved in DCM (75 mL), washed three times withwater (30 mL), dried over Na2SO4 and taken to dryness in vacuo. The crude product was purified byflash column chromatography (0%-40% CHCl3 in hexane), to give 12 as a white powder, (410 mg,0.93 mmol, 48% yield).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1,3-Diiodopropane(stabilized with Copper chip), other downstream synthetic routes, hurry up and to see.