Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 13421-13-1, name is 4-Chloro-2-iodobenzoic acid, This compound has unique chemical properties. The synthetic route is as follows., name: 4-Chloro-2-iodobenzoic acid
Sodium hydroxide (15.3g, 272mmol) in 180mL water solution of the 4- chloro-2-benzoic Acid iodide (15.4g, 54.5mmol), copper powder (0.346g, 5.5mmol), thiophenol (5.57mL, 54.5 It was placed mmol). After heating the reaction mixture solution to 120 C to proceed the reaction for 8 hours, it was passed through Celite and the filtered to remove the copper. While the mixed solution was filtered and stirred to progress after cooling to room temperature, it was added an excess of aqueous HCl solution (5M, 100mL). The resulting white solid was filtered and dried under reduced pressure after washing with excess water under reduced pressure to give the title compound as a white solid (13.7g, 95%).
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 13421-13-1.
Reference:
Patent; Dongwoo Fine-Chem.,Ltd.; Jo, Sung Hyun; Kim, Hyun Woo; (11 pag.)KR2015/15102; (2015); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com