Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 2043-53-0, name is 1-Iodo-1H,1H,2H,2H-perfluorodecane, This compound has unique chemical properties. The synthetic route is as follows., name: 1-Iodo-1H,1H,2H,2H-perfluorodecane
To a solution of 1H,1H,2H,2H-perfluoro-1-iododecane (8.0 g, 14 mmol) in dry ether (150 ml) at -78 C. under Ar was added t-BuLi (1.7 M in hexane; 35 ml, 21 mmol) dropwise with stirring. The mixture was stirred for 1.5 h at -78 C. and cholodiisopropylrosilane (1.7 ml, 10 mmol) was added to the reaction mixture dropwise. The mixture was stirred for 3 h and then warmed to ambient temperature. The reaction mixture was quenched with saturated NH4Cl aqueous solution and extracted with ether. The extract was dried over anhydrous MgSO4 and concentrated. The dark red liquid residue was passed through short column chromatography on silica gel with hexane to provide diisopropyl-1H,1H,2H,2H-perfluorodecanylsilane in 95% yield (5.3 g, 9.5 mmol) as a colorless liquid.
According to the analysis of related databases, 2043-53-0, the application of this compound in the production field has become more and more popular.
Reference:
Patent; University of Pittsburgh; US6897331; (2005); B2;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com