Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 2043-57-4, name is 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
In a 20 liter reaction vessel, 1500 g (3.16 mol) of 1H, 1H, 2H, 2H-perfluorohexylethyl iodide and 3 L of dimethylformamide were added, and 230 g (3.5 mol) of sodium azide was added. The mixture was stirred at room temperature for 3 h, GC showed complete conversion, selectivity 99%, water 3 L, allowed to stand, layered, the aqueous layer was washed three times with methyl tert-butyl ether,The three washed organic layers were washed three times with brine to give crude 1H, 1H, 2H, 2H-perfluorooctyl azide containing methyl tert-butyl ether.
According to the analysis of related databases, 2043-57-4, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Juhua Group Technology Center; Wang Zhiguang; Jiang Yun; (6 pag.)CN106278921; (2017); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com