Adding a certain compound to certain chemical reactions, such as: 375-80-4, name is 1,6-Diiodoperfluorohexane, belongs to iodides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 375-80-4, Computed Properties of C6F12I2
General procedure: In a typical procedure (IC2F4)2 (45.40g, 0.1mol) was dissolved in 100mL of acetonitrile and 200mL of water in a 500-mL round-bottomed flask. The solution was made basic with NaHCO3 (30.00g, 0.36mol) and then fresh Na2S2O4 (50.00g 0.28mmol, the ratio is 1:2.8) was slowly added with good stirring at 22C. After 20h, fluorine-19 NMR spectroscopy indicated the reaction was complete by disappearance of the -CF2I signal. The solution (NaSO2C2F4)2 and other byproducts are light yellow.
At the same time, in my other blogs, there are other synthetic methods of this type of compound, 1,6-Diiodoperfluorohexane, and friends who are interested can also refer to it.
Reference:
Article; Mei, Hua; Desmarteau, Darryl D.; Journal of Fluorine Chemistry; vol. 160; (2014); p. 12 – 15;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com