Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 16355-92-3, name is 1,10-Diiododecane, This compound has unique chemical properties. The synthetic route is as follows., Formula: C10H20I2
Example 19: Preparation of C10-bis-L-Lactate Diol (Compound 19b) [0135] 25.0 g 1,10-diiododecane (Compound 18b) was dissolved in 7 ml DCM, and the solution added to 120 g tetrabutylammonium-L-lactate (Compound 17b). The reaction mixture was placed in a 40C rotary evaporator bath, and rotated at top speed for 20 hours. The solution was then diluted with 100ml dichloromethane, and washed with 100 ml water. 750 ml diethyl ether were placed into a 2-liter Erlenmeyer flask and stirred magnetically. The lower organic phase from the separatory funnel was dripped into the diethyl ether with stirring until a precipitate appeared. The precipitated salt (tetrabutylammonium iodide) was vacuum-filtered through a medium porosity frit, and the filtrate was collected in a 1-liter round-bottom flask and washed once with 400 ml 1.25% sodium thiosulfate in water, and twice with 400 ml water. The ether layer was dried over anhydrous magnesium sulfate and the solvent was removed in vacuo to produce 15.5 g of the product. [0136] The structure of the product was confirmed by’H NMR.
According to the analysis of related databases, 16355-92-3, the application of this compound in the production field has become more and more popular.
Reference:
Patent; POLYMERIX CORPORATION; RUTGERS, THE STATE UNIVERSITY OF NEW JERSEY; WO2005/39489; (2005); A2;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com