Synthetic Route of 16355-92-3, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 16355-92-3, name is 1,10-Diiododecane, This compound has unique chemical properties. The synthetic route is as follows.
(3) Dissolve 2-methyl-4-aminoquinoline (4.75 g, 0.03 mol) in 100 mL of sulfolane, add 1,10-diiododecane (3.94 g, 0.01 mol), and raise the temperature to 80C to react 12h, lower the temperature, filter, wash the filter cake twice with water, wash the filter cake once with methanol, dry diquindine 8g, yield 56.7%, HPLC purity 81.5%;
The chemical industry reduces the impact on the environment during synthesis 1,10-Diiododecane. I believe this compound will play a more active role in future production and life.
Reference:
Patent; Wuhan Zhidun Science And Technology Co., Ltd.; Li Yaping; Xie Honglei; Zhang Ruipeng; Zhang Yixing; (8 pag.)CN111018777; (2020); A;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com