Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3032-81-3, name is 1,3-Dichloro-5-iodobenzene, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 3032-81-3
General procedure: [(Cinnamyl)PdCl]2 (5 mol percent) and AsPh3 (10 mol percent) were transferred into a vial (4 mL reaction volume) equipped with a septum, a small cannula and a stirring bar. After the vials were purged with argon, 1,4-dioxane distilled from sodium ketyl, 2 ml, iodobenzene (1 mmol), and HMDS (2 mmol) were injected into the vial by syringe. Then, the vial was placed in an alloy plate, which was transferred into a 300 mL autoclave of the 4560 series from Parr Instruments.(R). under argon atmosphere. After flushing the autoclave three times with CO, a pressure of 10 bar was adjusted and the reaction was performed for 16 h at 110 ¡ãC. Due to the sensitivity of the products no isolation was performed and characterization was done by GC-MS. Determination of the yield was done using the calibration factor of benzoyltrimethyl silane.
According to the analysis of related databases, 3032-81-3, the application of this compound in the production field has become more and more popular.
Reference:
Article; Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias; Tetrahedron Letters; vol. 53; 5; (2012); p. 582 – 584;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com