In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 217314-45-9, name is Methyl 3-amino-5-iodobenzoate belongs to iodides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. Recommanded Product: 217314-45-9
Step C: To a 0C solution of aniline from step B (21.7 g, 78.3 mmol) in 3:1 DCM:pyridine (75 mL) wasadded methanesulfonyl chloride (6.36 mL, 82.2 mmol). The ice bath was removed after 15 min and thesolution was stirred overnight at rt. The reaction mixture was extracted several times with IN HC1. Theorganic phase was dried, concentrated, and cliromatographed (1:1 EtOAc:Hex) to afford the desiredsulfonamide as a white solid.
The synthetic route of 217314-45-9 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; MERCK & CO., INC.; WO2006/2004; (2006); A1;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com