Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 60577-34-6, name is 4-Iodo-N-methylaniline, A new synthetic method of this compound is introduced below., Safety of 4-Iodo-N-methylaniline
(4) 7.7 g (33 mmol) of 4-iodo-N-methylaniline, 3.9 g (38 mmol) of acetic anhydride and 3.0 g (38 mmol) of pyridine,After reacting at room temperature for 1 hour, 50 ml of water was added to the reaction mixture, and the product was extracted with chloroform.After the reaction, usual post-treatment was performed to obtain 8.6 g of a yellow solid.This yellow solid was recrystallized using a mixed solvent of diethyl ether: ethanol = 5: 1 (v / v),7.6 g (84% yield) of 4-iodo-N-methylacetanilide was obtained as a yellow solid.
The synthetic route of 60577-34-6 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Unimatec Co., Ltd.; Saito, Satoshi; (9 pag.)JP5895454; (2016); B2;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com