Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 612-55-5, name is 2-Iodonaphthalene, This compound has unique chemical properties. The synthetic route is as follows., 612-55-5
General procedure: Benzo[d]thiazole (1.0 mmol), aryl iodide(1.5 mmol), CuFe2O4 nanoparticles (0.05 mmol), ligand (0.02 mmol), and base were (1.5-2 mmol) taken in solvent (3 mL) and heated at 110 oC, for 10 h. The progress of the reaction was monitored by TLC. After the reaction was complete CuFe2O4 nanoparticles were placed on the bottom of the flask by a neodymium magnet, and the supernatant solution was removed. The crude residue was extracted with ethyl acetate (3 10 mL). The combined organic layers were extracted with water, saturated brine solution, and dried over anhydrous Na2SO4. The organic layers were evaporated under reduced pressure and the resulting crude product was purified by column chromatography to give the corresponding 2-phenylbenzo[d]thiazole in excellent yields. The identity and purity of the product were confirmed by 1H, 13C NMR, and mass spectra.
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Reference:
Article; Satish; Reddy, K. Harsha Vardhan; Anil; Ramesh; Kumar, R. Uday; Nageswar; Tetrahedron Letters; vol. 56; 34; (2015); p. 4950 – 4953;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com