624-76-0, The chemical industry reduces the impact on the environment during synthesis 624-76-0, name is 2-Iodoethanol, I believe this compound will play a more active role in future production and life.
Compound 5 (1.41 g, 0.0043 mol) and potassium carbonate (1.78 g, 0.0129 mol) were added into a round bottom flask. The flask was made free of water and oxygen. The mixture was dissolved with DMF (60 ml). Then 2-iodo-ethanol (0.67 ml, 0.0086 mol) was slowly added dropwise. The reaction was raised to 50 C. and stirred. After completion of the reaction, the reaction was dissolved with ethyl acetate (250 ml), and then extracted with water (3¡Á60 ml) to remove DMF, and washed with saturated brine, dried with anhydrous magnesium sulfate, filtered, evaporated to dryness, and dried by pumping to provide a white solid 6 (1.475 g, 93.35%).
The chemical industry reduces the impact on the environment during synthesis 624-76-0. I believe this compound will play a more active role in future production and life.
Reference:
Patent; YANTAI UNIVERSITY; WANG, Hongbo; HONG, Xuechuan; ZHU, Xi; WANG, Pengyu; LV, Guangyao; FU, Jie; LUO, Huairong; ZHANG, Jianqiao; WEN, Meng; QU, Chunrong; ZHU, Jinmei; HU, Xianming; (7 pag.)US2016/102066; (2016); A1;,
Iodide – Wikipedia,
Iodide – an overview | ScienceDirect Topics – ScienceDirect.com